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Brand Name: Shanghai Sinofluoro Scientific Co., Ltd
Grade Standard: Medicine Grade
Type: Auxiliaries and Other Medicinal Chemicals
Place of Origin: China (Mainland)
MF: C24BF20.C19H15
CAS No.: 136040-19-2

Specifications


Alternate Name: triphenylcarbenium tetrakis(pentafluorophenyl) borate.

Physical Data: mp 180–182?°C.

Solubility: soluble in CH2Cl2, MeOH, and acetone, but its yellow color disappears because these solvents coordinate to the trityl salt.

Form Supplied in: yellow powder; commercially available from Asahi Glass Co. Ltd.

Analysis of Reagent Purity: NMR, mp.

Preparative Methods: trityl tetrakis(pentafluorophenyl)borate is prepared by mixing LiB(C6F5)4 and trityl chloride in hexane and refluxing overnight. It is prepared also by one-pot procedure starting from bromopentafluorobenzene.

Purification: recrystallization from CH2Cl2/hexane.

Handling, Storage, and Precautions: should be stored in a dry, dark, and cold place; stable at room temperature for long periods; does not decompose upon exposure to air.